Driven by global information technology and educational informationization, MOOC has become a key development direction of education. In order to improve the public service level, promote education equity and curriculum teaching reform, the Ministry of Education of China's "Opinions on accelerating the construction of high-level undergraduate education and comprehensively improving talent cultivation ability" points out that it is needed to vigorously promote MOOC and virtual simulation experiments, and vigorously promote and develop high-quality MOOC. Taking construction of building materials MOOC as an example, this paper has discussed high quality course resources construction from the following three aspects:basic situation and characteristics of building materials course, curriculum resources construction of building materials MOOC, and teaching design and effect analysis of building materials MOOC. The experience of course content, teaching resources, teaching mode and the precious experience of online appraisal are taken in this exploration, which lays practical foundation for the future MOOC construction of building materials and other subjects.