Gas loss is serious in current coal core method, and freezing core technology will become a new direction for gas content determination in the future, so it is the key to study gas desorption characteristics in low temperature environment (below 0℃). Therefore, in this paper, a self-made high/low temperature gas adsorption/desorption device is used to test gas desorption laws in low temperatures (-10, -20 and -30 ℃). The tested results show that the effect of temperature on gas desorption is very obvious. When temperature decreases, gas adsorption quantity increases; while gas desorption quantity decreases as temperature decreases. Lowering temperature suppresses gas desorption. And the lower the temperature is, the more obvious the gas desorption inhibitory effect is. Increasing gas pressure weakens gas desorption inhibitory effect in low temperature environment.